AQF-5000

Halogen and sulphur analysis

✓ Fully automated halogen and sulphur analysis

✓ Screening method for PFAS analysis

✓ Monitoring of quality criteria or limit values in quality assurance, process monitoring or environmental samples

✓ for liquid, solid and gaseous organic & inorganic samples

✓ Compliant with a wide range of standards and standard methods

✓ Fast measurement

 

Your advantages

Applicable to almost any sample matrix

Fast, robust and reliable: shorter measuring times thanks to parallel determination of fluorine, chlorine, bromine, iodine and sulphur in solid, liquid and gaseous samples

Significantly lower detection limits: than most conventional methods with better reproducibility of results

Compliance with standard norms: Compliant with a wide range of standards and standard methods

Measuring range: from ppb to the high percentage range

Resource protection

Coupling of hydropyrolysis and ion chromatography: saves valuable working time

Designed for longevity: robust workmanship, clear & simple handling, service and spare parts.

Sustainability: the system can be coupled with existing IC systems in the laboratory or connected to new IC systems specially designed for your samples. Manual systems that can be expanded at a later date can also be configured.

Minimal use of resources: thanks to the sturdy design, there is less wear and tear and parts rarely need to be replaced

Further development: the AQF-5000 is already the 4th generation of the coupling of sample digestion and ion chromatography (Combustion IC). More than 20 years of experience have gone into its development.

Easy handling

Complete automation: for liquid and solid samples

Possible samples: Solid, liquid, viscous and gaseous samples as well as LPG and LNG / organic and inorganic samples (including corrosive substances)

Easy cleaning and maintenance: thanks to the hinged oven

Additives that release the analytes from inorganic compounds can be used

A wide variety of applications: for example for

  • Chemistry,
  • Energy,
  • Environment,
  • Agriculture and food,
  • Heavy industry,
  • raw materials industry,
  • Petrochemistry,
  • pharmaceutical industry,
  • Consumer goods,
  • Waste & Recycling

Our service for you

4th generation of the combination of combustion digestion and ion chromatography as combustion IC. We provide the application know-how and optimize the Combustion IC for your application and ensure robust routine use.

Successful cooperation with ion chromatography specialists and the developer of the process, Nittoseiko Analytech

20 years of know-how for your analytical problem: Benefit from over 20 years of experience and knowledge. We can help you, regardless of whether you want a special application, already have a device, want to expand your system or have to cope with new application requirements.

Development support: for your method development

A system just for you: maximum flexibility thanks to modularity with other detectors and various autosamplers.
Comprehensive training: we support you in training your employees. This also applies to new employees, years after purchase

Also there for you after the purchase: many questions only arise during work. We are here to answer all your questions about the device and your measurement

Support and spare parts: we will be happy to help you, even in 10 years’ time

Application

Applications

This is a small selection of application examples:

  • AOF and EOF – sum parameters for the determination of fluorinated organics (PFAS) → find out more about PFAS here
  • Halogen content in electronic components (RoHS analysis, OLEDs)
  • Fluorine content in recycled materials from lithium batteries (black mass, lithium carbonate, electrolytes, anode and cathode materials)
  • Fluorine, chlorine and sulphur in primary and secondary energy sources
  • Basic materials and intermediate products of the glass industry
  • Fluorine and chlorine in heavy industry feedstocks
  • Halogen and sulphur content in waste/recycled materials
  • Halogen content in building materials
  • Halogen content in waste wood
  • Fluorine determination in textiles and other consumer goods

What does the Combustion IC measure?

The Combustion IC consists of the AQF-5000 hydropyrolytic digestion system and a directly coupled ion chromatograph. This enables the parallel determination of halogens (fluorine, chlorine, bromine and iodine) and sulphur in liquid, viscous, solid and gaseous samples. There are hardly any alternative methods available for fluorine analysis in particular.

Procedure of the AQF-5000

The AQF-5000 is a high-temperature digestion system that can be coupled with an ion chromatograph. The complete system is called a Combustion IC. The oxidative hydropyrolysis in the quartz glass or ceramic tube and the ion chromatographic determination of the analytes offer the highest degree of automation and accuracy.

For whom are the measurement results of the Combustion IC important?

The measurement results of the Combustion IC are important for anyone who wants to measure halogens, for example to monitor limit values in environmental analysis. The halogen content in petrochemical plants is also measured, for example to prevent corrosion in plants or to protect catalysts. Quality assurance, for example in chemical reactions where the halogen content in the product is monitored, and process monitoring are also typical areas of application.
The measurement results are important for companies, research facilities, universities, institutes, contract laboratories, but also for medium-sized companies and start-ups (e.g. battery recycling) in a wide range of sectors (chemicals, energy, environment, agriculture and food, heavy industry, raw materials industry, petrochemicals, pharmaceuticals, consumer goods, waste and recycling).

A reliable partner

No matter what your analytical problem is, we will work with you to find the best solution. We know how challenging regulations and compliance with limit values can be. Changes in political requirements, especially with regard to the new Drinking Water Ordinance and PFAS, place high demands on an analytical solution. We help you to find the best solution for you.

Control of the AQF-5000

Application-specific software for controlling combustion and absorption as well as optional detectors and feed systems

Standard methods

The AQF-5000 is fully compliant with the following relevant standard procedures, among others:

  • DIN 38409-59,
  • DIN EN 62321-3-2,
  • ISO 19242,
  • EN 17813,
  • ASTM D5987,
  • ASTM D7359,
  • ASTM D7994,
  • ASTM D8150,
  • ASTM D8247,
  • UOP 991,
  • UOP 1001

Measuring method

Work steps

  • Automatic sample feeding for gases, solids and liquids
  • Hydropyrolytic combustion digestion
  • Absorption of the combustion gases and automatic aliquoting/dilution of the absorption solution and transfer to the IC
  • Ion chromatographic detection of the analytes

Combustion digestion on the AQF-5000 enables the fully automated, simultaneous determination of fluorine, chlorine, bromine, iodine and sulphur using ion chromatography in almost all organic and inorganic substances. After digestion, absorption, oxidation/reduction and transfer to the IC, the halogens are analyzed as fluoride, chloride, bromide, iodide and sulphur as sulphate. The two systems (combustion and ion chromatography) work staggered and fully automatically without further manual intervention.

Sample preparation

In most applications, no further sample preparation is necessary. For particularly inhomogeneous samples, homogenization of the samples is necessary. Certain methods such as AOF or EOF require a sample preparation specified by the respective standard. We can offer you suitable sample preparation solutions.

Different autosamplers to suit your requirements

  • ABC-500: Semi-automatic autosampler for solid, viscous and liquid samples
  • ASC-570LS: Fully automatic sampler for solids and/or liquids (boat + syringe injection)
  • GI-520: Automatic sample feeding for gases and pre-vaporized LPG/LNG/CNG
  • GI-560: Direct feeding of LPG/LNG with automatic dosing and replica measurement

We are happy to help you put together the right components for your analysis.

Parameters

The following elements and parameters can be determined with the AQF-5000: Fluorine, chlorine, bromine, iodine, sulphur, AOF, EOF, AOCl, AOBr, AOI

Specifications

  • Furnace HF-500: Horizontal arrangement, up to 1100°C, automatic gas and combustion control depending on the sample matrix, furnace can be opened for easy access to the combustion tube.
  • Absorption module GA-500: absorption of combustion gases, constant volume function for determining the final volume of the absorption solution, sample dilution, transfer of an aliquot of the absorption solution to the IC
  • Measuring range: ppb to 100%
  • Gas supply: O299.7%; Ar ≥ 99.98%

Accessoires

FAQ

In combination with an ion chromatograph, the AQF-5000 measures the halogens fluorine, chlorine, bromine and iodine, sulphur and the parameters AOF, AOCl, AOBr, AOI and PFAS.

Organic and inorganic liquid, viscous, solid and gaseous samples are possible.

There is no typical application because the AQF-5000 is so versatile. Here are a few possible application examples:

  • AOF and EOF – sum parameters for the determination of fluorinated organics (PFAS) → find out more about PFAS here
  • Halogen content in electronic components (RoHS analysis, OLEDs)
  • Fluorine content in lithium batteries and their individual parts (production and recycling)
  • Fluorine, chlorine and sulphur in primary and secondary energy sources
  • Basic materials and intermediate products of the glass industry
  • Fluorine and chlorine in heavy industry feedstocks
  • Halogen and sulphur content in waste/recycled materials
  • Halogen content in building materials
  • Halogen content in waste wood
  • Fluorine determination in textiles and other consumer goods

Yes, the sum parameters for the determination of fluorinated organics(PFAS) can be measured with the Combustion IC.

The measurement results of the AQF-5000 are important for anyone who wants to measure halogens as an environmental parameter in order to comply with limit values. The halogen content in petrochemical plants is also measured in order to prevent corrosion, for example. Quality assurance, for example in chemical reactions where the halogen content in the product is monitored, and process monitoring are also typical areas of application. The measurement results are important for large companies, research facilities, universities, institutes, contract laboratories, but also for medium-sized companies and start-ups (e.g. battery recycling) in a wide range of sectors (chemicals, energy, environment, agriculture and food, heavy industry, raw materials industry, petrochemicals, pharmaceuticals, consumer goods, waste and recycling).

Yes, the C-IC delivers very precise and accurate results and can be used to monitor limit values.

The AQF-5000 is fully compliant with the following relevant standard procedures, among others:

DIN 38409-59, DIN EN 62321-3-2, ISO 19242, EN 17813, ASTM D5987, ASTM D7359, ASTM D7994, ASTM D8150, ASTM D8247, UOP 991, UOP 1001

The AQF-5000 is a high temperature digestion system that can be coupled to an ion chromatograph, referred to as a Combustion IC.

In most applications, no further sample preparation is necessary. For particularly inhomogeneous samples, homogenization of the samples is necessary. Certain methods such as AOF or EOF require a sample preparation specified by the respective standard. We can offer you suitable sample preparation modules for AOF, for example.

Yes, for example methods such as Wickbold, Schöninger or Druckbombe, but these are all very labor-intensive and do not deliver such reproducible results as the AQF-5000.

No, but we work together with specialists in the industry so that we can actively support the procurement of your ion chromatograph.

Yes, this is possible in most cases. We will be happy to advise you on the specific possibilities.

The measuring range is ppb to 100%.

The AQF-5000 works with oxygen, O299.7% and argon, Ar ≥ 99.98%

A device demonstration and test measurements on your samples are possible and useful.

Once your AQF-5000 has been installed, our service team will be available to provide you with detailed product training. Most questions will arise as you work, so we will also be able to help you with any questions that arise at a later date – at your premises or flexibly via an online meeting.

Advice and contact

Do you need more information?
Then please contact us by e-mail or telephone!

Or use the contact form and we will get back to you.

Consulting process

Get advice now - Contact us

Find the right elemental analyzer for your requirements. Our team of experts will support you in your selection and answer all your questions.

Use our contact form for a non-binding consultation or call us directly. We look forward to your inquiry!

Termine 2025

10. September 2025: Lab Supply Chemnitz
23. – 25. September 2025: Powtech Technopharm Nürnberg
24. September 2025: Lab Supply Leverkusen
8. Oktober 2025: Lab Supply Hamburg
12. November 2025: Lab Supply Augsburg

Dates 2025

September 10, 2025: Lab Supply Chemnitz
September 23 – 25, 2025: Powtech Technopharm Nuremberg
24. September 2025: Lab Supply Leverkusen
8. October 2025: Lab Supply Hamburg
12. November 2025: Lab Supply Augsburg